Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Elena Vinogradov; P. K. Madhu; Shimon Vega

doi:10.1016/S0009-2614(02)00060-X

Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Elena Vinogradov, P. K. Madhu, Shimon Vega

Research output: Contribution to journal › Article › peer-review

135 Scopus citations

Abstract

We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.

Original language	English (US)
Pages (from-to)	193-202
Number of pages	10
Journal	Chemical Physics Letters
Volume	354
Issue number	3-4
DOIs	https://doi.org/10.1016/S0009-2614(02)00060-X
State	Published - Mar 12 2002

ASJC Scopus subject areas

General Physics and Astronomy
Physical and Theoretical Chemistry

Access to Document

10.1016/S0009-2614(02)00060-X

Cite this

@article{a9861cb017694678a5c31cea14bba338,

title = "Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences",

abstract = "We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.",

author = "Elena Vinogradov and Madhu, {P. K.} and Shimon Vega",

note = "Funding Information: We thank financial support from the German–Israeli Foundation for Scientific Research and Development. The authors wish to thank Gil Goobes for his comparative study of the w-PMLG spectra of u--hystidine and natural abundant hystidine.",

year = "2002",

month = mar,

day = "12",

doi = "10.1016/S0009-2614(02)00060-X",

language = "English (US)",

volume = "354",

pages = "193--202",

journal = "Chemical Physics Letters",

issn = "0009-2614",

publisher = "Elsevier",

number = "3-4",

}

TY - JOUR

T1 - Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

AU - Vinogradov, Elena

AU - Madhu, P. K.

AU - Vega, Shimon

N1 - Funding Information: We thank financial support from the German–Israeli Foundation for Scientific Research and Development. The authors wish to thank Gil Goobes for his comparative study of the w-PMLG spectra of u--hystidine and natural abundant hystidine.

PY - 2002/3/12

Y1 - 2002/3/12

N2 - We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.

AB - We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.

UR - http://www.scopus.com/inward/record.url?scp=0037066031&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0037066031&partnerID=8YFLogxK

U2 - 10.1016/S0009-2614(02)00060-X

DO - 10.1016/S0009-2614(02)00060-X

M3 - Article

AN - SCOPUS:0037066031

SN - 0009-2614

VL - 354

SP - 193

EP - 202

JO - Chemical Physics Letters

JF - Chemical Physics Letters

IS - 3-4

ER -

Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Abstract

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this